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Mechanical properties and microstructure of multilayer graphene oxide cement mortar

《结构与土木工程前沿（英文）》 2021年 第15卷 第4期   页码 1058-1070 doi: 10.1007/s11709-021-0747-3

摘要： This study reports on the effects of multilayer graphene oxide (MGO) on compressive strength, flexural strength, and microstructure of cement mortar. The cement mortar was prepared with type P. II. 52.5 Portland cement, standard sand, and MGO. Four mixes were prepared with inclusion of MGO (0%, 0.02%, 0.04%, and 0.06% by weight of cement). The testing result shows that the compressive of GO-cement mortar increased by 4.84%–13.42%, and the flexural strength increased by 4.37%–8.28% at 3 d. GO-cement mortar’s compressive strength and flexural strength at 7 d increased by 3.84%–12.08% and 2.54%–13.43%, respectively. MGO made little contribution to the increases of compressive strength and flexural strength of cement mortar at 28 d. The results of X-ray diffraction (XRD), scanning electron microscope (SEM), and nitrogen (N2) adsorption/desorption tests show that the types of hydration products and crystal grain size did not change after adding MGO. Still, it can help to improve the microstructure of the cement mortar via regulating hydration products and can provide more condensed cores to accelerate hydration. Furthermore, the regulating action of MGO for the microstructure of cement mortar at an early age was better than that at 28 d.

关键词： graphene oxide     cement     mortar     mechanical properties     microstructure    

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ITZ microstructure, thickness, porosity and its relation with compressive and flexural strength of cementmortar; influence of cement fineness and water/cement ratio

《结构与土木工程前沿（英文）》 2022年 第16卷 第2期   页码 191-201 doi: 10.1007/s11709-021-0792-y

摘要： A new insight into the interfacial transition zone (ITZ) in cement mortar specimens (CMSs) that is influenced by cement fineness is reported. The importance of cement fineness in ITZ characterizations such as morphology and thickness is elucidated by backscattered electron images and by consequences to the compressive (Fc) and flexural strength (Ff), and porosity at various water/cement ratios. The findings indicate that by increasing the cement fineness the calcium silicate hydrate formation in the ITZ is favored and that this can refine the pore structures and create a denser and more homogeneous microstructure. By increasing cement fineness by about 25% of, the ITZ thickness of CMSs was reduced by about 30% and Fc was increased by 7%–52% and Ff by 19%–40%. These findings illustrate that the influence of ITZ features on the mechanical strength of CMSs is mostly related to the cement fineness and ITZ microstructure.

关键词： cement fineness     interfacial transition zone     compressive and flexural strength    

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Effect of embedment length of untreated natural fibres on the bond behaviour in cement mortar

Gudimella RAMAKRISHNA, Sriraman PRIYADHARSHINI

《结构与土木工程前沿（英文）》 2018年 第12卷 第4期   页码 454-460 doi: 10.1007/s11709-017-0454-2

摘要： The present investigation is focused on studying the effects of various matrices with 1:3, 1:4 and 1:5 mortars and fibre types of sisal and coir on the bond behavior at various ages of curing, i.e., 24 h, 3 d, 7 d and 28 d. The other parameters included in the investigation are water/cement (w/c) ratio, sand gradation and embedment length of fibres. In addition, the type of failure of sisal and coir fibres for different mixes of mortars at various curing ages is also reported. From the results, it is seen that the bond strength is improving with respect to age of curing in case of sisal fibres, but decreases in case of coir fibres. The failure of fibres due to fibre fracture is observed in sisal fibres and fibre pullout is observed in coir fibres. The other varying parameters such as mortar mixes, sand gradation, w/c ratio and embedded length also showed significant effect on bond behaviour of sisal and coir fibre with the cement mortar mixes.

关键词： bond strength     cement mortar     natural fibre     pullout test     type of failure    

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Silicon carbide waste as a source of mixture materials for cement mortar

Zhengwu Jiang, Qiang Ren, Haoxin Li, Qing Chen

《环境科学与工程前沿（英文）》 2017年 第11卷 第5期 doi: 10.1007/s11783-017-0974-y

摘要： This paper presents an investigation of the feasibility of recycling silicon carbide waste (SCW) as a source of mixture materials in the production of cement mortar. Mortars with SCW were prepared by replacing different amounts of cement with SCW, and the properties of the resulting mortars, such as the fluidity, strength and shrinkage, were studied in this work. Thermogravimetry-differential scanning calorimetry and scanning electron microscopy were employed to understand the reasons for the property changes of the mortars. The results indicate that SCW decreases the initial and 1-h fluidity of fresh mortar but improves the loss of fluidity. The mortar with SCW exhibits a lower strength at 3 d and 7 d but a higher strength at 28 d and 56 d compared to the control. The shrinkage rate of cement mortar with SCW shows an obvious decrease as the replacement ratio increases. In addition, the content of calcium hydroxide in hardened paste also shows that SCW has some impact on the hydration of the cement-SCW system. The microstructures of the hardened paste also show evidence for a later strength change of mortar containing SCW. This work provides a strategic reference for possibly applying SCW as a mixture material in the production of cement mortar.

关键词： Silicon carbide waste     Cement mortar     Fluidity     Strength     Shrinkage    

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Cement mortar with enhanced flexural strength and durability-related properties using

Qing LIU, Renjun LIU, Qiao WANG, Rui LIANG, Zongjin LI, Guoxing SUN

《结构与土木工程前沿（英文）》 2021年 第15卷 第1期   页码 99-108 doi: 10.1007/s11709-021-0721-0

摘要： The low flexural strength and high brittleness of cementitious materials impair their service life in building structures. In this study, we developed a new polymer-modified mortar by polymerization of acrylamide (AM) monomers during the cement setting, which enhanced the flexural and durable performances of mortars. The mechanical properties, micro-and-pore structures, hydrated products, interactions between cement hydrates and polyacrylamide (PAM), and durability-related properties of the mortars were investigated comprehensively. Mortars with 5% PAM exhibited the best performance in terms of flexural strength among all the mixtures. The mechanical strength of cement pastes modified by polymerization of AM monomers was significantly superior to those modified by PAM. The chemical interactions between the polymer molecules and cement hydrates together with the formation of polymer films glued the cement hydrates and polymers and resulted in an interpenetrating network structure, which strengthened the flexural strength. Reductions in porosity and calcium hydroxide content and improvement in capillary water absorption were achieved with the addition of PAM. Finally, the chloride resistance was significantly enhanced with the incorporation of PAM.

关键词： acrylamide     in situ polymerization     interaction     porosity     durability    

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Acid-treated carbon nanotubes and their effects on mortar strength

M. ELKASHEF,K. WANG,M. N. ABOU-ZEID

《结构与土木工程前沿（英文）》 2016年 第10卷 第2期   页码 180-188 doi: 10.1007/s11709-015-0325-7

摘要： In the present study, multi-walled carbon nanotubes (MWCNTs) were treated in an acidic mixture solution, made with nitric and sulfuric acids in a ratio of 3:1 by volume. The durations of the treatment were 100 and 180 min. The defects of these treated MWCNTs were examined using Raman spectroscopy. The attachment of hydroxyl functional groups to the walls of the MWCNTs were verified using FTIR spectroscopy. The dispersion of CNTs with acid treatment is assessed using UV-Vis spectroscopy and Scanning Electron Microscopy (SEM). The results indicate that the duration of the acid treatment has significant effect on both the degree of defects and functionality of the MWCNT. The compressive strength of mortar increased with the addition of the acid-treated MWCNTs; however, no appreciable difference was noted for the two treatment durations under this study.

关键词： carbon nanotubes     concrete     composites     nanomaterials     cement    

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Effect of fineness of ash on pozzolanic properties and acid resistance of sugarcane bagasse ash replaced cement

Shan E ALI; Rizwan AZAM; Muhammad Rizwan RIAZ; Mohamed ZAWAM

《结构与土木工程前沿（英文）》 2022年 第16卷 第10期   页码 1287-1300 doi: 10.1007/s11709-022-0872-7

摘要： This paper addresses the potential use of Sugar Cane Bagasse Ash (SCBA) as a pozzolanic material for partial cement replacement in concrete mixtures. Cement mortars containing SCBA having five different particle size distributions at a replacement rate of 20% by weight were used to study the chemical and physical pozzolanic properties of SCBA. The durability of SCBA replaced mortars was also evaluated. SCBA with 0% retained on sieve No. 325 was used to replace 20% by weight of cement and create mortar specimens that were subjected to sulfuric acid attack of varying concentrations (1%−3% by weight of water). The tested samples were observed to check visual distortion, mass loss, and compressive strength loss at 1, 7, 14, 28, and 56 d of acidic exposure, and the results were compared to those for the control sample, that was lime water cured, at the same ages. The SCBA sets were found to meet the requirements for pozzolan class N specified by ASTM C 618. Mortars containing SCBA with 0% or 15% retention produced better compressive strength than the control mortars after 28 d. Additionally, X-ray fluorescence and X-ray diffraction analysis showed that the SCBA had favorable chemical properties for a pozzolanic material. Furthermore, SCBA replaced samples at all ages showed improved resistance against acidic attack relative to that of the control mortars. Maximum deterioration was seen for 3% concentrated solution. This study’s findings demonstrated that SCBA with an appropriate fineness could be used as a pozzolanic material, consistently with ASTM C 618.

关键词： durability     cement replacement     sugarcane bagasse ash     fineness of ash     pozzolanic properties     mortar acid resistance    

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水中爆炸对围岩增耦的实验研究

王占江,蔡宗义,郑学锋,朱玉荣

《中国工程科学》 2009年 第11卷 第4期   页码 46-49

摘要：

为研究水中爆炸对围岩的增耦，在一个直径1.6 m的水泥砂浆半球体装置上，将其中心预留的直径0.3 m的腔室内注水和置入水泥砂浆芯体，对比性地进行了一系列的1.00 g TNT （2,4,6—三硝基甲苯）当量的填实和空腔爆炸实验。水泥砂浆球表运动测量数据表明，与水泥砂浆中的空腔解耦相比，水中空腔爆炸的解耦效果较差，尤其水腔中爆炸可大大增强爆炸能量的耦合。可以推断，水下爆炸会明显增强围岩中的爆炸应力波强度，近水域中的空中爆炸也可能会增强围岩中的爆炸能耦合，因而相对于围岩和堤坝中同距离、同药量的爆炸来讲，所引起

关键词： 水下爆炸     围岩增耦     水泥砂浆     应力波     空腔解耦    

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Experimental investigation on concrete overlaid with textile reinforced mortar: Influences of mix, temperature

《结构与土木工程前沿（英文）》 2023年 第17卷 第2期   页码 271-283 doi: 10.1007/s11709-022-0896-z

摘要： Textile reinforced mortar is widely used as an overlay for the repair, rehabilitation, and retrofitting of concrete structures. Recently, textile reinforced concrete has been identified as a suitable lining material for improving the durability of existing concrete structures. In this study, we developed a textile-reinforced mortar mix using river sand and evaluated the different characteristics of the textile-reinforced mortar under various exposure conditions. Studies were carried out in two phases. In the first phase, the pullout strength, temperature resistance, water absorption, and compressive and bending strength values of three different textile-reinforced mortar mixes with a single type of textile reinforcement were investigated. In the second phase, the chemical resistance of the mix that showed the best performance in the abovementioned tests was examined for use as an overlay for a concrete substrate. Investigations were performed on three different thicknesses of the textile reinforced mortar overlaid on concrete specimens that were subjected to acidic and alkaline environments. The flexural responses and degradations of the textile reinforced mortar overlaid specimens were examined by performing bending tests. The experimental findings indicated the feasibility of using textile reinforced mortar as an overlay for durable concrete construction practices.

关键词： textile reinforced mortar     bending tests     acid and alkaline environment     concrete overlay    

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Extending blending proportions of ordinary Portland cement and calcium sulfoaluminate cement blends:

《结构与土木工程前沿（英文）》 2021年 第15卷 第5期   页码 1249-1260 doi: 10.1007/s11709-021-0770-4

摘要： This study extended blending proportion range of ordinary Portland cement (OPC) and calcium sulfoaluminate (CSA) cement blends, and investigated effects of proportions on setting time, workability, and strength development of OPC-CSA blend-based mixtures. Thermogravimetric analysis (TGA) and X-ray diffraction (XRD) were conducted to help understand the performance of OPC-CSA blend-based mixtures. The setting time of the OPC-CSA blends was extended, and the workability was improved with increase of OPC content. Although the early-age strength decreased with increase of OPC content, the strength development was still very fast when the OPC content was lower than 60% due to the rapid formation and accumulation of ettringite. At 2 h, the OPC-CSA blend-based mortars with OPC contents of 0%, 20%, 40%, and 60% achieved the unconfined compressive strength (UCS) of 17.5, 13.9, 9.6, and 5.0 MPa, respectively. The OPC content had a negligible influence on long-term strength. At 90 d, the average UCS of the OPC-CSA blend-based mortars was 39.2 ± 1.7 MPa.

关键词： calcium sulfoaluminate cement     cement blends     hydration reaction     setting     workability     compressive strength    

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Experimental study and assessment of thermal energy storage mortar with paraffin/recycled brick powder

Luchen HAO; Jianzhuang XIAO; Wanzhi CAO; Jingting SUN

《结构与土木工程前沿（英文）》 2022年 第16卷 第10期   页码 1301-1314 doi: 10.1007/s11709-022-0883-4

摘要： Thermal energy storage recycled powder mortar (TESRM) was developed in this study by incorporating paraffin/recycled brick powder (paraffin/BP) composite phase change materials (PCM). Fourier transform infrared and thermogravimetric analysis results showed that paraffin/BP composite PCM had good chemical and thermal stability. The onset melting temperature and latent heat of the composite PCM were 46.49 °C and 30.1 J·g−1. The fresh mortar properties and hardened properties were also investigated in this study. Paraffin/BP composite PCM with replacement ratio of 0%, 10%, 20%, and 30% by weight of cement were studied. The results showed that the static and dynamic yield stresses of TESRM were 699.4% and 172.9% higher than those of normal mortar, respectively. The addition of paraffin/BP composite PCM had a positive impact on the mechanical properties of mortar at later ages, and could also reduce the dry shrinkage of mortar. The dry shrinkage of TESRM had a maximum reduction about 26.15% at 120 d. The thermal properties of TESRM were better than those of normal mortar. The thermal conductivity of TESRM was 36.3% less than that of normal mortar and the heating test results showed that TESRM had good thermal energy storage performance.

关键词： recycled powder mortar     recycled brick powder     thermal energy storage     paraffin     phase change material    

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Study of bond strength between various grade of Ordinary Portland Cement (OPC) and Portland PozzolaneCement (PPC) mixes and different diameter of TMT bars by using pullout test

A D POFALE, S P WANJARI

《结构与土木工程前沿（英文）》 2013年 第7卷 第1期   页码 39-45 doi: 10.1007/s11709-013-0193-y

摘要： Since last two decades, the Portland Pozzolane Cement (PPC) is extensively used in structural concrete. But, till to date, a few literature is available on bond strength of concrete using PPC mixes. There are many literatures available on bond strength of concrete mixes using Ordinary Portland Cement (OPC). Hence, a comparative study was conducted on bond strength between OPC and PPC mixes. In the present investigation, total 24 samples consisting of M20, M35 and M50 grades of concrete and 16 and 25 mm diameter of TMT bar were tested for 7 and 28 days. The pullout bond test was conducted on each specimen as per IS: 2770-1967/1997 [1] and the results were observed at 0.25 mm slip at loaded end called as critical bond stress and at maximum bond load called as maximum bond stress. It was observed that the critical bond strength of PPC mixes is 10% higher than OPC mixes. Whereas, marginal improvement was noticed in maximum bond strength of PPC mixes. Hence, based on these findings, it could be concluded that development length for PPC mixes could be reduced by 10% as compared with same grade of OPC mixes.

关键词： bond strength     Portland Pozzolane Cement (PPC) concrete     Ordinary Portland Cement (OPC) concrete     bond between concrete and steel     pullout test     development length    

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Autogenous healing mechanism of cement-based materials

《结构与土木工程前沿（英文）》   页码 948-963 doi: 10.1007/s11709-023-0960-3

摘要： Autogenous self-healing is the innate and fundamental repair capability of cement-based materials for healing cracks. Many researchers have investigated factors that influence autogenous healing. However, systematic research on the autogenous healing mechanism of cement-based materials is lacking. The healing process mainly involves a chemical process, including further hydration of unhydrated cement and carbonation of calcium oxide and calcium hydroxide. Hence, the autogenous healing process is influenced by the material constituents of the cement composite and the ambient environment. In this study, different factors influencing the healing process of cement-based materials were investigated. Scanning electron microscopy and optical microscopy were used to examine the autogenous healing mechanism, and the maximum healing capacity was assessed. Furthermore, detailed theoretical analysis and quantitative detection of autogenous healing were conducted. This study provides a valuable reference for developing an improved healing technique for cement-based composites.

关键词： autogenous healing     cement-based materials     healing mechanism     aggregation effect    

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Research review of the cement sand and gravel (CSG) dam

Xin CAI, Yingli WU, Xingwen GUO, Yu MING

《结构与土木工程前沿（英文）》 2012年 第6卷 第1期   页码 19-24 doi: 10.1007/s11709-012-0145-y

摘要： The cement sand and gravel (CSG) dam is a new style of dam that owes the advantages both of the concrete faced rock-fill dam (CRFD) and roller compacted concrete (RCC) gravity dam, because of which it has attracted much attention of experts home and abroad. At present, some researches on physic-mechanical property of CSG material and work behavior of CSG dam have been done. This paper introduces the development and characteristics of CSG dam systematically, and summarizes the progress of the study on basic tests, constitutive relation of CSG material and numerical analysis of CSG dam, in addition, indicates research and application aspect of the dam.

关键词： cement sand and gravel (CSG) dam     cement sand and gravel (CSG) material     research review    

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Experimental study on behavior of mortar-aggregate interface after elevated temperatures

Wan WANG, Jianzhuang XIAO, Shiying XU, Chunhui WANG

《结构与土木工程前沿（英文）》 2017年 第11卷 第2期   页码 158-168 doi: 10.1007/s11709-016-0374-6

摘要： A push-out test program was designed and conducted to study the meso-scale behavior of mortar-aggregate interface for concrete after elevated temperatures ranging from 20°C to 600°C with the concept of modeled concrete (MC) and modeled recycled aggregate concrete (MRAC). The MCs and MRACs were designed with different strength grade of mortar and were exposed to different elevated temperatures. Following that the specimens were cooled to room temperature and push-out tests were conducted. Failure process and mechanical behaviors were analyzed based on failure modes, residual load-displacement curves, residual peak loads and peak displacements. It is found that failure modes significantly depended on specimen type, the elevated temperature and the strength grade of mortar. For MC, major cracks started to propagate along the initial cracks caused by elevated temperatures at about 80% of residual peak load. For MRAC, the cracks appeared at a lower level of load with the increasing elevated temperatures. The cracks connected with each other, formed a failure face and the specimens were split into several parts suddenly when reaching the residual peak load. Residual load-displacement curves of different specimens had similarities in shape. Besides, effect of temperatures and strength grade of mortar on residual peak load and peak displacement were analyzed. For MC and MRAC with higher strength of new hardened mortar, the residual peak load kept constant when the temperature is lower than 400°C and dropped by 43.5% on average at 600°C. For MRAC with lower strength of new hardened mortar, the residual peak load began to reduce when the temperatures exceeded 200°C and reduced by 27.4% and 60.8% respectively at 400°C and 600°C. The properties of recycled aggregate concrete (RAC) may be more sensitive to elevated temperatures than those of natural aggregate concrete (NAC) due to the fact that the interfacial properties of RAC are lower than those of NAC, and are deteriorated at lower temperatures.

关键词： mortar-aggregate interface     push-out test     elevated temperatures     modeled concrete (MC)     modeled recycled aggregate concrete (MRAC)    

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标题 作者 时间 类型 操作

Mechanical properties and microstructure of multilayer graphene oxide cement mortar

期刊论文

ITZ microstructure, thickness, porosity and its relation with compressive and flexural strength of cementmortar; influence of cement fineness and water/cement ratio

期刊论文

Effect of embedment length of untreated natural fibres on the bond behaviour in cement mortar

Gudimella RAMAKRISHNA, Sriraman PRIYADHARSHINI

期刊论文

Silicon carbide waste as a source of mixture materials for cement mortar

Zhengwu Jiang, Qiang Ren, Haoxin Li, Qing Chen

期刊论文

Cement mortar with enhanced flexural strength and durability-related properties using

Qing LIU, Renjun LIU, Qiao WANG, Rui LIANG, Zongjin LI, Guoxing SUN

期刊论文

Acid-treated carbon nanotubes and their effects on mortar strength

M. ELKASHEF,K. WANG,M. N. ABOU-ZEID

期刊论文

Effect of fineness of ash on pozzolanic properties and acid resistance of sugarcane bagasse ash replaced cement

Shan E ALI; Rizwan AZAM; Muhammad Rizwan RIAZ; Mohamed ZAWAM

期刊论文

水中爆炸对围岩增耦的实验研究

王占江,蔡宗义,郑学锋,朱玉荣

期刊论文

Experimental investigation on concrete overlaid with textile reinforced mortar: Influences of mix, temperature

期刊论文

Extending blending proportions of ordinary Portland cement and calcium sulfoaluminate cement blends:

期刊论文

Experimental study and assessment of thermal energy storage mortar with paraffin/recycled brick powder

Luchen HAO; Jianzhuang XIAO; Wanzhi CAO; Jingting SUN

期刊论文

Study of bond strength between various grade of Ordinary Portland Cement (OPC) and Portland PozzolaneCement (PPC) mixes and different diameter of TMT bars by using pullout test

A D POFALE, S P WANJARI

期刊论文

Autogenous healing mechanism of cement-based materials

期刊论文

Research review of the cement sand and gravel (CSG) dam

Xin CAI, Yingli WU, Xingwen GUO, Yu MING

期刊论文

Experimental study on behavior of mortar-aggregate interface after elevated temperatures

Wan WANG, Jianzhuang XIAO, Shiying XU, Chunhui WANG

期刊论文